1,4-Thiazepane-1,1-dione hydrochloride → HCID 71735093, Verbindung
Reaktionsgleichung
C(OC(N1CC[N:11]([CH2:14][C:15]2[CH:20]=[CH:19][C:18]([C@@H:21]3[O:30][C:25]4=[N:26][CH:27]=[CH:28][CH:29]=[C:24]4[O:23][CH2:22]3)=[CH:17][CH:16]=2)[CH2:10][CH2:9]1)=O)(C)(C)C.[S:31]1(=[O:39])(=[O:38])[CH2:37][CH2:36][CH2:35]NCC1>>[O:38]=[S:31]1(=[O:39])[CH2:37][CH2:36][CH2:35][N:11]([CH2:14][C:15]2[CH:20]=[CH:19][C:18]([C@@H:21]3[O:30][C:25]4=[N:26][CH:27]=[CH:28][CH:29]=[C:24]4[O:23][CH2:22]3)=[CH:17][CH:16]=2)[CH2:10][CH2:9]1Komponenten
3
Versuchsvorschrift
Compound 275 is synthesized from Intermediate C and [1,4]thiazepane 1,1-dioxide according to General Method H. (LC/MS method 16: ES+ m/z 375.4 [M+H]+, Rt=2.51 min)
Quellen und Nachweise
- ORD-Eintrag
- ord-7a2387b72aa84d62bb71f6d4073578d7
- Quelldatensatz
- uspto-grants-2015_02