Aluminium lithium hydride → 2-(1-Benzothiophen-2-yl)ethan-1-amine

Beteiligte Stoffe

Reaktionsschritte

Using analogous reaction conditions and workup as described in Example 1, step 2, 2-(2-nitro-vinyl)-benzo[b]thiophene (I-9a: 2.1 g, 0.010 mol) in dry THF (30 mL) was reacted with LAH (0.81 g, 0.021 mol) in dry THF (20 mL) to afford 1.6 g of the product (87.91% yield).

Herkunft & Nachweise