Methoxyacetic Acid → 2-(methoxymethyl)-4-methyl-1H-benzo[d]imidazol-6-ol
Reaktionsgleichung
[NH2:1][C:2]1[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([CH3:9])[C:7]=1[NH2:8].[CH3:11][O:12][CH2:13][C:14](O)=O>>[CH3:11][O:12][CH2:13][C:14]1[NH:1][C:2]2[CH:3]=[C:4]([OH:10])[CH:5]=[C:6]([CH3:9])[C:7]=2[N:8]=1Komponenten
3
Versuchsvorschrift
0.55 g (4.00 mmol) 3,4-diamino-5-methyl-phenol and 1.57 mL (20.00 mmol) methoxy-acetic acid were stirred for 1 h at 120° C. Then the reaction mixture was evaporated down and further reacted as crude product.
Aufarbeitung
- customThen the reaction mixture was evaporated down
- customfurther reacted as crude product
Quellen und Nachweise
- ORD-Eintrag
- ord-0a9782ae3d6c474b9a96289133f1de66
- Quelldatensatz
- uspto-grants-2015_02
- Patentnummer
- US08952014B2
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