HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride → 6-[2-(2,6-Dimethyl-morpholin-4-yl)-ethoxy]-2-thieno[3,2-c]pyridin-6-yl-chromen-4-one oxime, hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride | HCID 12955539 | — |
| Edukt | 6-Hydroxy-2-thieno[3,2-c]pyridin-6-yl-chromen-4-one O-tert-butyl-oxime | HCID 86673101 | — |
| Produkt | 6-[2-(2,6-Dimethyl-morpholin-4-yl)-ethoxy]-2-thieno[3,2-c]pyridin-6-yl-chromen-4-one oxime, hydrochloride | HCID 137187585 | — |
Reaktionsschritte
6-[2-(2,6-Dimethyl-morpholin-4-yl)-ethoxy]-2-thieno[3,2-c]pyridin-6-yl-chromen-4-one oxime, hydrochloride was prepared in 48% overall yield using the method described in example 127, starting from 6-Hydroxy-2-thieno[3,2-c]pyridin-6-yl-chromen-4-one O-tert-butyl-oxime (example 127B) and 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride (JACS 1949, 500-505; US2006/14948).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08962627B2 |
| Quelldatensatz | uspto-grants-2015_02 |
| ORD ID | ord-359e4d5998dd4f5dbb5d57634467f503 |
| Quellennotiz | uspto-grants-2015_02 |