HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diisopropylamine → HCID 23346036, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diisopropylamine | HCID 7912 | — |
| Edukt | p-Phenylene diisothiocyanate | HCID 19958 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | HCID 23346036 | HCID 23346036 | — |
Reaktionsschritte
To a solution of 1.92 g. of 1,4-phenylenediisothiocyanate in 100 ml. of acetonitrile is added 2.5 g. of diisopropylamine. On standing, a precipitate forms which is filtered off and crystallized from acetone-cyclohexane to yield 2.7 g. of the title compound, melting point 185° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04218396 |
| Quelldatensatz | uspto-grants-1980_08 |
| ORD ID | ord-eb2cf8b6e22245c39b51d070cdc91d54 |
| Quellennotiz | uspto-grants-1980_08 |