Phosphate → 2-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-benzothiazole-6-thiol
Reaktionsgleichung
[CH3:1][O:2][C:3]([NH:5][C:6]1[S:7][C:8]2[C:14]([CH3:15])=[C:13]([S:16]C#N)[CH:12]=[C:11]([CH:19]([CH3:21])[CH3:20])[C:9]=2[N:10]=1)=[O:4].SC[C@H]([C@@H](CS)O)O.P([O-])([O-])([O-])=O>CCO>[CH3:1][O:2][C:3]([NH:5][C:6]1[S:7][C:8]2[C:14]([CH3:15])=[C:13]([SH:16])[CH:12]=[C:11]([CH:19]([CH3:21])[CH3:20])[C:9]=2[N:10]=1)=[O:4]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The title compound was prepared according to General Method 14 using 2-(methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole (1.5 g, 4.7 mmol), dithiothreitol (2.9 g, 18.7 mmol), EtOH (50 mL), and phosphate buffer (15 mL). MS (APCI): 296 (M−H).
Quellen und Nachweise
- ORD-Eintrag
- ord-2c30a77d2f2c4e1397f30357085b1649
- Quelldatensatz
- uspto-grants-2003_03
- Patentnummer
- US06528510B1
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