HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Amino-4-methoxybenzanilide → 4-Methoxy-N-phenyl-3-[3-(4-sulfamoyl-phenyl)-thioureido]-benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Amino-4-methoxybenzanilide | HCID 8426 | — |
| Edukt | 4-Isothiocyanatobenzenesulfonamide | HCID 521359 | — |
| Produkt | 4-Methoxy-N-phenyl-3-[3-(4-sulfamoyl-phenyl)-thioureido]-benzamide | HCID 9846872 | 47% |
Reaktionsschritte
Prepared according to the procedure described for Example 60 using 3-amino-4-methoxy-N-phenyl-benzamide (0.974 g, 4.01 mmol) and 4-isothiocyanatobenzenesulfonamide (0.858 g, 4.00 mmol) to afford the product (0.858 g); m.p. 193-195° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06528528B2 |
| Quelldatensatz | uspto-grants-2003_03 |
| ORD ID | ord-451df6bf59164eb3a4eaa2b594d21be1 |
| Quellennotiz | uspto-grants-2003_03 |