Sodium Hydroxide → 4'-Dimethoxymethylbiphenyl-4-carboxylic acid

HRID 1860008Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1860008
[CH3:1][O:2][CH:3]([O:20][CH3:21])[C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:15]=[CH:14][C:13]([C:16]([O:18]C)=[O:17])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1.[OH-].[Na+]>>[CH3:21][O:20][CH:3]([O:2][CH3:1])[C:4]1[CH:5]=[CH:6][C:7]([C:10]2[CH:15]=[CH:14][C:13]([C:16]([OH:18])=[O:17])=[CH:12][CH:11]=2)=[CH:8][CH:9]=1

Komponenten

3

Edukt 2

HCID 14798Sodium HydroxideHCID 18625704Methyl 4'-dimethoxymethylbiphenyl-4-carboxylate

Produkt 1

HCID 186256964'-Dimethoxymethylbiphenyl-4-carboxylic acidAusbeute 100,1 %

Versuchsvorschrift

In a similar manner to that described in Example 2, a reaction was carried out using methyl 4′-dimethoxymethylbiphenyl-4-carboxylate (1.89 g), which is the product of Reference example 11(a), and aqueous sodium hydroxide (1N, 9.90 ml) and the reaction mixture was treated to afford the desired compound (1.80 g) as colorless crystals.

Aufarbeitung

  1. additionthe reaction mixture was treated

Quellen und Nachweise

ORD-Eintrag
ord-082edb70c69f4c4d9be86f4b0f653062
Quelldatensatz
uspto-grants-2003_03
Patentnummer
US06528525B1

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