Sodium Hydroxide → 4-(2-hydroxyphenyl)benzoic Acid

HRID 1860020Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1860020
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:13]=[CH:12][C:11]([C:14]([O:16]C)=[O:15])=[CH:10][CH:9]=1.[OH-].[Na+]>>[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:13]=[CH:12][C:11]([C:14]([OH:16])=[O:15])=[CH:10][CH:9]=1

Komponenten

3

Edukt 2

HCID 14798Sodium HydroxideHCID 45648562-(4-Methoxycarbonylphenyl)phenol

Produkt 1

HCID 106562444-(2-hydroxyphenyl)benzoic AcidAusbeute 92,9 %

Versuchsvorschrift

In a similar manner to that described in Example 2, a reaction was carried out using methyl 2′-hydroxybiphenyl-4-carboxylate (498 mg) and aqueous sodium hydroxide (1N, 4.81 ml) and the reaction mixture was treated to afford the title compound (434 mg) as colorless crystals.

Aufarbeitung

  1. additionthe reaction mixture was treated

Quellen und Nachweise

ORD-Eintrag
ord-340d1ef9824643168ccac76c4eb8a5ab
Quelldatensatz
uspto-grants-2003_03
Patentnummer
US06528525B1

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