HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dichlorocinnamic acid → (R)-1-[(E)-3-(3,4-Dichloro-phenyl)-acryloyl]-2-methyl-[1,4]diazepan-5-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dichlorocinnamic acid | HCID 688027 | — |
| Edukt | (R)-2-methyl-[1,4]diazepan-5-one | HCID 28064214 | — |
| Produkt | (R)-1-[(E)-3-(3,4-Dichloro-phenyl)-acryloyl]-2-methyl-[1,4]diazepan-5-one | HCID 68432228 | — |
Reaktionsschritte
In analogy to the procedure described in intermediate 78C, (E)-3,4-dichlorocinnamic acid and (R)-2-methyl-[1,4]diazepan-5-one gave the title compound as a colorless gum, MS: m/e=327.3 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07632829B2 |
| Quelldatensatz | uspto-grants-2009_12 |
| ORD ID | ord-8141f72d1a7e473faea850fcd678cc96 |
| Quellennotiz | uspto-grants-2009_12 |