HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dichlorocinnamic acid → (Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-6-methyl-[1,4]diazepan-5-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dichlorocinnamic acid | HCID 688027 | — |
| Edukt | 6-Methyl-1,4-diazepan-5-one hydrochloride | HCID 68434983 | — |
| Produkt | (Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-6-methyl-[1,4]diazepan-5-one | HCID 68432289 | — |
Reaktionsschritte
In analogy to the procedure described in intermediate 78C, (E)-3,4-dichlorocinnamic acid and 6-methyl-[1,4]diazepan-5-one hydrochloride gave the title compound as a colorless gum, MS: 327.1 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07632829B2 |
| Quelldatensatz | uspto-grants-2009_12 |
| ORD ID | ord-d5ecb3da94114dcea2c2af6b1d8127fb |
| Quellennotiz | uspto-grants-2009_12 |