Phenylacetic Acid → N'-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-phenylacetohydrazide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Phenylacetic Acid	HCID 999	—
Edukt	N'-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-cyclohexylacetohydrazide	HCID 57979752	—
Produkt	N'-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-phenylacetohydrazide	HCID 57979739	47%

Reaktionsschritte

The title compound (42 mg, 47%) as a white foam was prepared from 2-phenylacetic acid (41 mg, 0.3 mmol) and 1-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3)hydrazine (66 mg, 0.2 mmol) according to the procedures described for N′-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-cyclohexylacetohydrazide (Example 7A). HPLC/MS (method A): retention time =3.30 min, (M+H)+=449.2.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US07632837B2
Quelldatensatz	uspto-grants-2009_12
ORD ID	ord-44260eb49b47412380db6d9c2e723457
Quellennotiz	uspto-grants-2009_12