HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Bromo-2-methyl-1-propene → 5,7-Dimethoxy-3-methyl-1-naphthol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Bromo-2-methyl-1-propene | HCID 357785 | — |
| Edukt | N,N-diethyl-3,5-dimethoxybenzamide | HCID 4075317 | — |
| Edukt | HCID 178454970 | HCID 178454970 | — |
| Produkt | 5,7-Dimethoxy-3-methyl-1-naphthol | HCID 15404113 | 50% |
Reaktionsschritte
5,7-Dimethoxy-3-methyl-1-naphthol is synthesized from N,N-diethyl-3,5-dimethoxybenzamide and 3-bromo-2-methylpropene according to the method described by Sibi et al. (J. Org. Chem. 1986, Vol. 51, pp. 271-273). The yield is approximately 50%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06096246 |
| Quelldatensatz | uspto-grants-2000_08 |
| ORD ID | ord-ef76600b6f3440a9a463417d54c86752 |
| Quellennotiz | uspto-grants-2000_08 |