HCID 18689938, Verbindung → HCID 18689941, Verbindung

HRID 1871923Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1871923
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]=[C:12]1[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]1>C(O)C.[C].[Pd]>[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH2:11][CH:12]1[CH2:13][CH2:14][NH:15][CH2:16][CH2:17]1

Komponenten

4

Edukt 1

HCID 18689938HCID 18689938, Verbindung

Produkt 1

HCID 18689941HCID 18689941, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 178418390HCID 178418390, VerbindungKatalysatorHCID 702EthanolLösungsmittel

Versuchsvorschrift

4-(2-Quinolylmethylene)piperidine (9.62 g) was dissolved in ethanol (500 ml), and 10% palladium-carbon (1.9 g) was added to the solution. The mixture was stirred under a hydrogen stream at room temperature for 90 minutes. After removal of the catalyst by filtration, the filtrate was concentrated under reduced pressure, to thereby obtain the title compound as a colorless solid.

Aufarbeitung

  1. customAfter removal of the catalyst
  2. filtrationby filtration
  3. concentrationthe filtrate was concentrated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-1028fdb0ad1a4cc5b26e5373dedba277
Quelldatensatz
uspto-grants-2000_08
Patentnummer
US06107308

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