Morpholine, 4-chloro- → 4-n-Butyl-2-methoxy-5 chlorobenzoic acid
Reaktionsgleichung
[CH2:1]([C:5]1[CH:13]=[CH:12][C:8]([C:9]([OH:11])=[O:10])=[C:7]([O:14][CH3:15])[CH:6]=1)[CH2:2][CH2:3][CH3:4].[Cl:16]N1CCOCC1>>[CH2:1]([C:5]1[C:13]([Cl:16])=[CH:12][C:8]([C:9]([OH:11])=[O:10])=[C:7]([O:14][CH3:15])[CH:6]=1)[CH2:2][CH2:3][CH3:4]Komponenten
3
Versuchsvorschrift
4-n-Butyl-2-methoxybenzoic acid (0.5 g; 2.9 mmol) and N-chloromorpholine (356 mg; 2.9 mmol) were treated in a similar manner to that described in Preparation 24 to give the title compound as a white soid (0.4 g).
Aufarbeitung
- customdescribed in Preparation 24
Quellen und Nachweise
- ORD-Eintrag
- ord-f73aa7e27772481e9fa24b9935f4ecaa
- Quelldatensatz
- uspto-grants-2000_08
- Patentnummer
- US06110934
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