Ammonia → 3-(Tridecylamino)propionamide

HRID 1872798Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1872798
[CH2:1]([NH:14][CH2:15][CH2:16][C:17]([O:19]C)=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[NH3:21]>>[CH2:1]([NH:14][CH2:15][CH2:16][C:17]([NH2:21])=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Komponenten

3

Edukt 2

HCID 222AmmoniaHCID 18687169Methyl 3-tridecylaminopropionate

Produkt 1

HCID 186872443-(Tridecylamino)propionamide

Versuchsvorschrift

A solution of methyl 3-(tridecylamino)propionate (0.77 g) in 10N-methanolic ammonia (7 ml) was allowed to stand at room temperature for 7 days. The resultant crystal was collected by filtration and washed with a small portion of methanol to give 3-(tridecylamino)propionamide (0.16 g).

Aufarbeitung

  1. filtrationThe resultant crystal was collected by filtration
  2. washwashed with a small portion of methanol

Quellen und Nachweise

ORD-Eintrag
ord-5019b1eefeff4ea1a2e544b5029cc1d9
Quelldatensatz
uspto-grants-2000_08
Patentnummer
US06110933

Notizen zur Reaktion

Wird geladen…