Methyl iodide → HCID 68590834, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[C:7]2[S:8][CH:9]=[CH:10][C:6]=2[CH2:5][CH2:4][N:3]=1.[CH3:11][I:12]>C(OCC)(=O)C>[I-:12].[CH3:11][N+:3]1[CH2:4][CH2:5][C:6]2[CH:10]=[CH:9][S:8][C:7]=2[C:2]=1[CH3:1]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A mixture of 4.64 g (31 mmol) 7-methyl-4,5-dihydro-thieno[2,3-c]pyridine (prepared analogously to J.Am.Chem.Soc., 1951, 1257), 8.0 ml (128 mmol) methyl iodide and 20 ml of ethyl acetate is stirred for 15 min. The precipitate formed is suction filtered, washed with ethyl acetate and dried in vacuo.
Aufarbeitung
- customprepared analogously to J.Am.Chem.Soc
- customThe precipitate formed
- filtrationfiltered
- washwashed with ethyl acetate
- customdried in vacuo
Quellen und Nachweise
- ORD-Eintrag
- ord-0843bf2fcfc94ff0ada02d33864cdc05
- Quelldatensatz
- uspto-grants-2012_11
- Patentnummer
- US08309542B2
Notizen zur Reaktion
Wird geladen…