Hydrochloric Acid → HCID 69203826, Verbindung

HRID 1875553Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1875553
[CH3:1][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([O:10]C)=[O:9])[CH3:3].[ClH:18]>>[ClH:18].[CH3:3][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([OH:10])=[O:9])[CH3:1]

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 23144875HCID 23144875, Verbindung

Produkt 1

HCID 69203826HCID 69203826, Verbindung

Reaktionsbedingungen

Temperatur
100 °C

Versuchsvorschrift

The mixture of methyl 3-dimethylaminomethyl-2-nitrobenzoate (0.72 g) and 6M hydrochloric acid was stirred at 100° C. overnight. After cooling the mixture to room temperature, the precipitated crystals were filtered out, washed with diethylether and dried under reduced pressure to obtain 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride.

Aufarbeitung

  1. temperatureAfter cooling the mixture to room temperature
  2. filtrationthe precipitated crystals were filtered out
  3. washwashed with diethylether
  4. customdried under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-bd892fdec45446f8a5fee6d5f6191d21
Quelldatensatz
uspto-grants-2012_11
Patentnummer
US08309561B2

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