HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-(2,4-Dichlorophenyl)-2-methyl-3-furaldehyde → Cyclohexyl[5-(2,4-dichlorophenyl)-2-methyl-3-furyl]methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-(2,4-Dichlorophenyl)-2-methyl-3-furaldehyde | HCID 83595757 | — |
| Edukt | HCID 178420632 | HCID 178420632 | — |
| Produkt | Cyclohexyl[5-(2,4-dichlorophenyl)-2-methyl-3-furyl]methanol | HCID 68511587 | 77% |
Reaktionsschritte
An operation similar to that in Example 3 (2) was performed using 5-(2,4-dichlorophenyl)-2-methyl-3-furaldehyde (1.3 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (7.5 mL) to give the title compound (1.3 g, 77%) as a white crystal.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08309580B2 |
| Quelldatensatz | uspto-grants-2012_11 |
| ORD ID | ord-85cadfcc69ef4610a00e4d6ba7420bfb |
| Quellennotiz | uspto-grants-2012_11 |