HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-(4-Fluoro-2-methylphenyl)-2-methyl-3-furaldehyde → Cyclohexyl[5-(4-fluoro-2-methylphenyl)-2-methyl-3-furyl]methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-(4-Fluoro-2-methylphenyl)-2-methyl-3-furaldehyde | HCID 86646367 | — |
| Edukt | HCID 178420632 | HCID 178420632 | — |
| Produkt | Cyclohexyl[5-(4-fluoro-2-methylphenyl)-2-methyl-3-furyl]methanol | HCID 68515490 | 72% |
Reaktionsschritte
An operation similar to that in Example 3 (2) was performed using 5-(4-fluoro-2-methylphenyl)-2-methyl-3-furaldehyde (2.6 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (18 mL) to give the title compound (2.6 g, 72%) as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08309580B2 |
| Quelldatensatz | uspto-grants-2012_11 |
| ORD ID | ord-16a088323c3a4b889b0e46625ec3144b |
| Quellennotiz | uspto-grants-2012_11 |