HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-(4-Chloro-2-methylphenyl)-2-methyl-3-furaldehyde → [5-(4-Chloro-2-methylphenyl)-2-methyl-3-furyl] (cyclohexyl)methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-(4-Chloro-2-methylphenyl)-2-methyl-3-furaldehyde | HCID 86646368 | — |
| Lösungsmittel | HCID 178420632 | HCID 178420632 | — |
| Produkt | [5-(4-Chloro-2-methylphenyl)-2-methyl-3-furyl] (cyclohexyl)methanol | HCID 68514219 | 156,4% |
Reaktionsschritte
An operation similar to that in Example 3 (2) was performed using 5-(4-chloro-2-methylphenyl)-2-methyl-3-furaldehyde (1.6 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (10 mL) to give the title compound (1.7 g, 77%) as a white crystal.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08309580B2 |
| Quelldatensatz | uspto-grants-2012_11 |
| ORD ID | ord-190b2a545df64902b5ffe700b3d0a12f |
| Quellennotiz | uspto-grants-2012_11 |