Thionyl Chloride → HCID 68515497, Verbindung

HRID 1877062Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1877062
[CH3:1][CH:2]([CH3:18])[CH2:3][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])O.S(Cl)([Cl:21])=O>C1(C)C=CC=CC=1>[Cl:21][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])[CH2:3][CH:2]([CH3:18])[CH3:1]

Komponenten

4

Edukt 2

HCID 24386Thionyl ChlorideHCID 685095783-Methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol

Produkt 1

HCID 68515497HCID 68515497, VerbindungAusbeute 100 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

To a solution of 3-methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol (1.5 g) in toluene (20 mL) was added thionyl chloride (0.9 mL), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (1.6 g, 100%) as an oil.

Aufarbeitung

  1. customThe solvent was evaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-059cce386ae5449980b3c2710eff9d05
Quelldatensatz
uspto-grants-2012_11
Patentnummer
US08309580B2

Notizen zur Reaktion

Wird geladen…