HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2'-Aminoacetophenone → HCID 178450482, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2'-Aminoacetophenone | HCID 11086 | — |
| Edukt | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Produkt | HCID 178450482 | HCID 178450482 | — |
Reaktionsschritte
A mixture of ethyl 2-butyryl-3-ethoxyacrylate (23.5 g, 0.11 mol) and 2'-aminoacetophenone (13.5 g, 0.1 mol) was warmed on a steam bath for 10 minutes. Crystallisation from petroleum ether gave ethyl 2-butyryl-3-(2-acetylphenylamino)acrylate as a mixture of E/Z isomers (14.9 g, 49%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05143920 |
| Quelldatensatz | uspto-grants-1992_09 |
| ORD ID | ord-18a5463c6df942f88a2780cefe61fa27 |
| Quellennotiz | uspto-grants-1992_09 |