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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1886003Erstellt: 25. Oktober 2026

Trifluoroacetic acid → HCID 178481704, Verbindung

https://huagongshe.com/reaction/1886003

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTrifluoroacetic acidHCID 6422—
EduktTrifluoroacetyl fluorideHCID 67716—
EduktN-MethylhydrazinecarbothioamideHCID 2723853—
ProduktHCID 178481704HCID 178481704—

Reaktionsschritte

This exemplified compound may be readily synthesized by the reaction of methyl isocyanate with hydrazine to give 4-methyl-3-thiosemicarbazide followed by cyclocondensation with trifluoroacetic acid as described in U.S. Pat. No. 4,477,459. This compound may also be prepared by the reaction of 4-methyl-3-thiosemicarbazide with trifluoroacetylfluoride and heat (U.S. Pat. No. 3,780,052).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05149620
Quelldatensatzuspto-grants-1992_09
ORD IDord-b98c545d21194b3c89942f661b4ae0d1
Quellennotizuspto-grants-1992_09