Trifluoroacetic acid → 2-(12-Phthalimido dodecyl)propane dioic acid

HRID 1886746Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1886746
C([O:5][C:6](=[O:38])[CH:7]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][N:27]1[C:31](=[O:32])[C:30]2=[CH:33][CH:34]=[CH:35][CH:36]=[C:29]2[C:28]1=[O:37])[C:8]([O:10]C(C)(C)C)=[O:9])(C)(C)C.FC(F)(F)C(O)=O>ClCCl>[C:28]1(=[O:37])[N:27]([CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH:7]([C:6]([OH:38])=[O:5])[C:8]([OH:10])=[O:9])[C:31](=[O:32])[C:30]2=[CH:33][CH:34]=[CH:35][CH:36]=[C:29]12

Komponenten

4

Edukt 2

HCID 6422Trifluoroacetic acidHCID 866489122-(12-Phthalimido dodecyl)propane dioic acid di-tert-butyl ester

Produkt 1

HCID 866489112-(12-Phthalimido dodecyl)propane dioic acidAusbeute 100 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel

Versuchsvorschrift

Following general procedure D, 16.0 mmol (8.45 g) of 5c and 160 mmol (11.9 mL) of trifluoroacetic acid were reacted in 12 mL of dichloromethane at room temperature and the mixture was processed. Yield 100%.

Quellen und Nachweise

ORD-Eintrag
ord-2c5e79c602a84d9fa0caec80d5c30337
Quelldatensatz
uspto-grants-2013_08
Patentnummer
US08501199B2

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