HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzenesulfonyl chloride, 3,4-dichloro- → N-(2-benzoyl-4-chloro-phenyl)-3,4-dichloro-benzenesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzenesulfonyl chloride, 3,4-dichloro- | HCID 7383 | — |
| Edukt | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| Produkt | N-(2-benzoyl-4-chloro-phenyl)-3,4-dichloro-benzenesulfonamide | HCID 11247684 | — |
Reaktionsschritte
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 115 mg of (2-amino-5-chloro-phenyl)-phenyl-methanone and 123 mg of 3,4-Dichloro-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 7.25 (d, 1H, J=8.8 Hz), 7.36-39 (m, 3H), 7.43-47 (m, 3H), 7.53 (dd, 1H, J=8.8 Hz, 2.4 Hz), 7.61 (m, 1H), 7.65 (m, 1H), 7.73 (d, 1H, J=8.8 Hz), 9.56 (s, 1H). MS: m/z 440.7 (M++1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07741519B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-b0bd93ef82ba4277b77e5c9ef6beaa1a |
| Quellennotiz | uspto-grants-2010_06 |