HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chloro-phenyl)-4-butyl-benzenesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| Edukt | 4-Butylbenzene-1-sulfonyl chloride | HCID 2737352 | — |
| Produkt | N-(2-benzoyl-4-chloro-phenyl)-4-butyl-benzenesulfonamide | HCID 11166253 | — |
Reaktionsschritte
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 115 mg of (2-amino-5-chloro-phenyl)-phenyl-methanone and 116 mg of 4-butyl-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 0.90 (t, 3H, J=6.8 Hz), 1.29 (m, 2H), 1.46 (m, 2H), 2.49 (t, 2H, J=7.6 Hz), 7.05 (d, 2H, J=8.4 Hz), 7.32 (d, 1H, J=2.4 Hz), 7.40 (m. 4H), 7.47 (dd, 1H, J=8.8 Hz, 2.8 Hz), 7.56 (m, 3H), 7.76 (d, 1H, J=8.8 Hz), 9.78 (s, 1H). MS: m/z 428.9 (M++1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07741519B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-a3768d3827464801be7bee201bf28881 |
| Quellennotiz | uspto-grants-2010_06 |