HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Amino-5-bromobenzophenone → N-(2-benzoyl-4-bromo-phenyl)-4-tert-butyl-benzenesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Amino-5-bromobenzophenone | HCID 99677 | — |
| Edukt | 4-t-Butylbenzenesulfonyl chloride | HCID 139882 | — |
| Produkt | N-(2-benzoyl-4-bromo-phenyl)-4-tert-butyl-benzenesulfonamide | HCID 11259990 | — |
Reaktionsschritte
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 138 mg of (2-Amino-5-bromo-phenyl)-phenyl-methanone and 116 mg of 4-tert-butyl-benzenesulfonyl chloride 1H-NMR (400 MHz, CDCl3): δ 1.21 (s, 9H), 7.30 (d, 2H, J=8.8 Hz), 7.36-7.44 (m, 4H), 7.47 (d, 1H, J=2.4 Hz), 7.54-7.63 (m, 4H), 7.21 (d, 1H, J=8.8 Hz), 9.92 (s, 1H). MS: m/z 473.4 (M++1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07741519B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-36888cfef7c94e86937e0acf614c103d |
| Quellennotiz | uspto-grants-2010_06 |