2-Chlorophenol → 2-Chlorophenyl sulfamate

Reaktionsgleichung

C1([O:4][S:5](=[O:8])(=[O:7])[NH2:6])CC1.[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[OH:16]>>[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[NH:6][S:5](=[O:8])(=[O:7])[O-:4].[Cl:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[O:16][S:5](=[O:7])(=[O:4])[NH2:6]

Komponenten

Edukt 2

HCID 72452-Chlorophenol

HCID 57785190Cyclopropyl sulfamate

Produkt 2

HCID 216944982-Chlorophenyl sulfamate

HCID 866327882-Chlorophenylsulfamate

Versuchsvorschrift

2-Chlorophenylsulfamate was synthesized according to the method presented in the synthesis of Sulfamic acid cyclopropyl ester in Example 1 with the exception of utilizing 2-chlorophenol to obtain sulfamic acid 2-chloro-phenyl ester.

Quellen und Nachweise

ORD-Eintrag: ord-be894a248944428f8694eca828bd3ac7
Quelldatensatz: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08513186B2

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