1-Ethylcyclopropanol → Sulfamic acid 1-ethyl-cyclopropyl ester

Reaktionsgleichung

[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=[CH:5]C=[CH:3][CH:2]=1.C(C1(O)CC1)C>>[CH2:6]([C:1]1([O:7][S:8](=[O:10])(=[O:11])[NH2:9])[CH2:2][CH2:3]1)[CH3:5]

Komponenten

Edukt 2

HCID 5450931-Ethylcyclopropanol

HCID 11030308Phenylsulfamate

Produkt 1

HCID 57785622Sulfamic acid 1-ethyl-cyclopropyl ester

Versuchsvorschrift

Sulfamic acid 1-ethyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-ethylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234) to obtain sulfamic acid 1-ethyl-cyclopropyl ester.

Aufarbeitung

customSulfamic acid 1-ethyl-cyclopropyl ester was synthesized

Quellen und Nachweise

ORD-Eintrag: ord-3ff2c911b282439eb26b9ebf49e5138b
Quelldatensatz: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08513186B2

Notizen zur Reaktion

Wird geladen…