Hydrochloric Acid → HCID 86594427, Verbindung

Reaktionsgleichung

[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH:13]C(OC(C)(C)C)=O)[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8].[ClH:22]>>[ClH:22].[ClH:22].[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH2:13])[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8]

Komponenten

Edukt 2

HCID 313Hydrochloric Acid

HCID 86594426HCID 86594426, Verbindung

Produkt 1

HCID 86594427HCID 86594427, Verbindung

Versuchsvorschrift

(S)-2-tert-Butoxycarbonylamino-4-[(2-methoxyethyl)-methylamino]-butyric acid methyl ester (0.086 g, 0.28 mmol) was treated with HCl (1 mL of 4M in dioxane) and sonicated. The mixture was concentrated and dried under high vacuum to provide the product.

Aufarbeitung

customsonicated
concentrationThe mixture was concentrated
customdried under high vacuum
customto provide the product

Quellen und Nachweise

ORD-Eintrag: ord-c61b1ba44a41445485bcc6c9346e342e
Quelldatensatz: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08518983B2

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