HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thiophosgene → 2-Chloro-4-methylphenyl isothiocyanate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thiophosgene | HCID 10040 | — |
| Edukt | 2-Chloro-p-toluidine | HCID 12007 | — |
| Edukt | Diisopropylethylamine | HCID 81531 | — |
| Produkt | 2-Chloro-4-methylphenyl isothiocyanate | HCID 143529 | 58,3% |
Reaktionsschritte
The title compound was prepared following the procedure described for intermediate-2 using 2-chloro-4-methyl aniline (2.0 g, 14.00 mmol), thiophosgene (1.62 g, 14.00 mmol) and N-ethyl di-isopropyl amine (3.63 g, 28.00 mmol) to afford 1.5 g of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08519149B2 |
| Quelldatensatz | uspto-grants-2013_08 |
| ORD ID | ord-3b59b75f740b42dfa65e357b2132c9af |
| Quellennotiz | uspto-grants-2013_08 |