HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Aluminium lithium hydride → 3-(8-Phenyloctyloxy)-2-hydroxypropylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Aluminium lithium hydride | HCID 21226445 | — |
| Edukt | 3-(8-Phenyloctyloxy)-2-hydroxypropylazide | HCID 21474713 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 3-(8-Phenyloctyloxy)-2-hydroxypropylamine | HCID 21474729 | 88,7% |
Reaktionsschritte
A procedure similar to that described in Preparation 13 was repeated, except that 2.6 g of 3-(8-phenyloctyloxy)-2-hydroxypropylazide (prepared as described in Preparation 65), 0.65 g of lithium aluminum hydride and 80 ml of anhydrous tetrahydrofuran were used, to give 2.11 g of the title compound, melting at 50° C. to 54° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05578620 |
| Quelldatensatz | uspto-grants-1996_11 |
| ORD ID | ord-c4eb1dabbc3c407ba96253284616737e |
| Quellennotiz | uspto-grants-1996_11 |