Methylhydrazine → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

HRID 1902139Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1902139
Cl[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3].[CH3:17][NH:18][NH2:19]>CO>[CH3:17][NH:18][NH:19][C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3]

Komponenten

4

Edukt 2

HCID 6061MethylhydrazineHCID 540353651-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Cloroformate

Produkt 1

HCID 544690901-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

The title compound is prepared by reacting the compound of Example 27 (1 mole) with methylhydrazine (1.1 mole) in methanol.

Quellen und Nachweise

ORD-Eintrag
ord-b50d9ee2a7eb4b859e89f04fdbfd22bb
Quelldatensatz
uspto-grants-1996_11
Patentnummer
US05578731

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