Methyl carbazate → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Hydrazinocarbonylhydrazinecarboxylate

HRID 1902141Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1902141
[C:1]([O:5][CH:6]1[CH2:11][C:10]([CH3:13])([CH3:12])[N:9]([O:14][CH3:15])[C:8]([CH3:17])([CH3:16])[CH2:7]1)(=[O:4])[NH:2][NH2:3].[C:18](OC)(=[O:21])[NH:19][NH2:20]>CO>[NH:19]([C:18]([NH:3][NH:2][C:1]([O:5][CH:6]1[CH2:7][C:8]([CH3:17])([CH3:16])[N:9]([O:14][CH3:15])[C:10]([CH3:12])([CH3:13])[CH2:11]1)=[O:4])=[O:21])[NH2:20]

Komponenten

4

Edukt 2

HCID 80519Methyl carbazateHCID 536527591-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Carbazate

Produkt 1

HCID 542840721-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Hydrazinocarbonylhydrazinecarboxylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

The title compound is prepared by reacting the compound of Example 28 (1 mole) with methyl carbazate (1 mole) by refluxing the reaction mixture in methanol.

Quellen und Nachweise

ORD-Eintrag
ord-6a81b3c8785341339b9eb3eca665aab3
Quelldatensatz
uspto-grants-1996_11
Patentnummer
US05578731

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