N-Allyl-2,2'-iminodiethanol → N-[2-(2-Methoxyethoxy)ethyl]diethanolamine
Reaktionsgleichung
[CH2:1]([N:4]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7])[CH:2]=C.S(C1C=CC(C)=CC=1)([O:14][CH2:15][CH2:16][O:17][CH2:18]COC)(=O)=O>>[CH3:18][O:17][CH2:16][CH2:15][O:14][CH2:2][CH2:1][N:4]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7]Komponenten
3
Versuchsvorschrift
The title compound was prepared as described above for N-allyldiethanolamine in Example 1 except that 2-methoxyethoxyethyl tosylate was used (0.55 mol, 150.9 g) in a 0.5 mol preparation. The pure diol whose formula is shown below was obtained (49.8 g, 48%) on fractional distillation at 129°-131° C. (0.04 mm):
Aufarbeitung
- customin a 0.5 mol preparation
- custombelow was obtained (49.8 g, 48%)
- distillationon fractional distillation at 129°-131° C. (0.04 mm)
Quellen und Nachweise
- ORD-Eintrag
- ord-00593ba9d30d4b0892dcb3dd130175ef
- Quelldatensatz
- uspto-grants-1984_03
- Patentnummer
- US04436664
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