Hydrochloric Acid → 4-Amino-3-hydroxy-6-methyl-1-phenylheptane hydrochloride

HRID 1906363Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1906363
C(OC([NH:8][CH:9]([CH2:20][CH:21]([CH3:23])[CH3:22])[CH:10]([OH:19])[CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=O)(C)(C)C.[ClH:24]>CO>[ClH:24].[NH2:8][CH:9]([CH2:20][CH:21]([CH3:23])[CH3:22])[CH:10]([OH:19])[CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 138931534-t-Butyloxycarbonylamino-3-hydroxy-6-methyl-1-phenylheptane

Produkt 1

HCID 200441484-Amino-3-hydroxy-6-methyl-1-phenylheptane hydrochloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

The resultant compound of Example 1 (87 mg, 0.27 mmol) was dissolved in methanol (1 ml) and was treated with methanolic HCl (5 ml of 0.75M). After 15 hours the solution was evaporated to provide the desired compound as a glass (71 mg) which was used without further purification.

Aufarbeitung

  1. customAfter 15 hours the solution was evaporated

Quellen und Nachweise

ORD-Eintrag
ord-906dd61b2f37435788b58d762f0e206a
Quelldatensatz
uspto-grants-1987_03
Patentnummer
US04652551

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