HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl alpha-acetamidocinnamate → Acetylphenylalanine methyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl alpha-acetamidocinnamate | HCID 340163 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Acetylphenylalanine methyl ester | HCID 704002 | 82,4% |
Reaktionsschritte
A second recycling of the catalyst is performed under the conditions described above, but introducing methyl α-acetamidocinnamate (1.6 g) and ethyl acetate (10 cc). Pure N-acetylphenylalanine methyl ester (1.33 g) is thus obtained with a conversion of 100%, its rotatory power being:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04654176 |
| Quelldatensatz | uspto-grants-1987_03 |
| ORD ID | ord-e343201433b347ff99acb0176de1801c |
| Quellennotiz | uspto-grants-1987_03 |