HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Mepp → 1-[(6-Chloro-3-methoxyquinoxalin-2-yl)aminocarbonyl]-4-(2-methylphenyl)piperazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Mepp | HCID 91965 | — |
| Edukt | ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69241674 | — |
| Produkt | 1-[(6-Chloro-3-methoxyquinoxalin-2-yl)aminocarbonyl]-4-(2-methylphenyl)piperazine | HCID 69243768 | 89% |
Reaktionsschritte
Ethyl N-(6-chloro-3-methoxyquinoxalin-2-yl)carbamate and 1-(2-methylphenyl)piperazine were reacted by the same way with the example 106 to obtain the titled compound (yield, 89%). H NMR (300 MHz, CDCl3): δ 2.35 (s, 3H), 3.01 (s, 4H), 3.76 (s, 4H), 4.14 (s, 3H), 7.03-7.52 (m, 6H), 7.68-7.77 (m, 2H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08598173B2 |
| Quelldatensatz | uspto-grants-2013_12 |
| ORD ID | ord-0fdacc8c79aa47078e7fef4b14f87e8c |
| Quellennotiz | uspto-grants-2013_12 |