Silica → N-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamide

HRID 1912241Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1912241
C[CH2:2][CH2:3][CH2:4][N:5]([C:10]([NH:12][C:13]([C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1)=[O:14])=[S:11])[CH2:6][CH2:7][CH2:8]C.[Si](=O)=O>>[CH3:8][CH2:7][CH2:6][N:5]([C:10]([NH:12][C:13]([C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1)=[O:14])=[S:11])[CH2:4][CH2:3][CH3:2]

Komponenten

3

Edukt 2

HCID 24261SilicaHCID 12357718N-(dibutylcarbamothioyl)-3,4,5-trimethoxybenzamide

Produkt 1

HCID 12357717N-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamide

Versuchsvorschrift

A mixture of 90 parts by mass of PET obtained above and 10 parts by mass of silicon dioxide (“Silysia 445,” average particle size 2.5 μm, manufactured by Fuji Silysia Chemical Ltd.) was kneaded at 260° C. using a vented counter-rotation twin-axis extruder (L/D=35) with 30 mmφ, to prepare a PPT master (MS-4) containing 10% by mass of silicon dioxide.

Aufarbeitung

  1. customwas kneaded at 260° C.

Quellen und Nachweise

ORD-Eintrag
ord-349e197454b24492b94b51c9c718043d
Quelldatensatz
uspto-grants-2013_12
Patentnummer
US08609227B2

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