HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine → 4-(4-(3-Pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine | HCID 22041340 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-(4-(3-Pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine | HCID 22041328 | — |
Reaktionsschritte
The mixture containing 2-nitro-4-(4-(3-pyridyl)pyrimidin-2-yloxy)phenylamine in methanol with catalytic amount of 10% Pd/C was hydrogenated until disappearance of yellow color to yield 4-(4-(3-pyridyl)pyrimidin-2-yloxy)benzene-1,2-diamine. MS: MH+=279.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08614330B2 |
| Quelldatensatz | uspto-grants-2013_12 |
| ORD ID | ord-8ed5c1b25eb64513822f2276de211d21 |
| Quellennotiz | uspto-grants-2013_12 |