Potassium Carbonate → Ethyl 4-(benzyloxy)-3-hydroxybenzoate

HRID 1918318Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1918318
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([O:19]C(=O)C)[CH:6]=1)[CH3:2].C(=O)([O-])[O-].[K+].[K+]>CO>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][C:8]([O:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[C:7]([OH:19])[CH:6]=1)[CH3:2]

Komponenten

4

Edukt 2

HCID 11430Potassium CarbonateHCID 67170201HCID 67170201, Verbindung

Produkt 1

HCID 11311797Ethyl 4-(benzyloxy)-3-hydroxybenzoate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

The compound of step 2 (10 g, 31.8 mmol) was dissolved in methanol, potassium carbonate (88 mg, 0.636 mmol) was added and the mixture was stirred for 2 h under reflux. The solution was evaporated to dryness and the residue used without further purification.

Aufarbeitung

  1. temperatureunder reflux
  2. customThe solution was evaporated to dryness
  3. customthe residue used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-8b32513e163d4143a66e1a137d6b959b
Quelldatensatz
uspto-grants-2013_12
Patentnummer
US08618304B2

Notizen zur Reaktion

Wird geladen…