N-Methyloxan-4-amine--hydrogen chloride (1/1) → Imidazole-1-sulfonic acid methyl-(tetrahydro-pyran-4-yl)-amide

HRID 1928777

Reaktionsgleichung

Reaktionsgleichung von HRID 1928777
Cl.[CH3:2][NH:3][CH:4]1[CH2:9][CH2:8][O:7][CH2:6][CH2:5]1.FC(F)(F)S([O-])(=O)=O.[N:18]1([S:23](N2C=C[NH+](C)C2)(=[O:25])=[O:24])[CH:22]=[CH:21][N:20]=[CH:19]1>>[CH3:2][N:3]([CH:4]1[CH2:9][CH2:8][O:7][CH2:6][CH2:5]1)[S:23]([N:18]1[CH:22]=[CH:21][N:20]=[CH:19]1)(=[O:25])=[O:24]

Komponenten

3

Edukt 2

HCID 22736998N-Methyloxan-4-amine--hydrogen chloride (1/1)HCID 866341663-(1H-Imidazol-1-ylsulfonyl)-1-methyl-1H-imidazolium trifluoromethanesulfonate

Produkt 1

HCID 68913796Imidazole-1-sulfonic acid methyl-(tetrahydro-pyran-4-yl)-amide

Versuchsvorschrift

Imidazole-1-sulfonic acid methyl-(tetrahydro-pyran-4-yl)-amide was prepared in accordance with step A of the general method described in example 76 from methyl-(tetrahydro-pyran-4-yl)amine hydrochloride and 3-(1H-imidazol-1-ylsulfonyl)-1-methyl-1H-imidazolium trifluoromethanesulfonate; MS: m/e=246.8 (M+H+).

Quellen und Nachweise

ORD-Eintrag
ord-b6ee7d822a374602895fe005c5cdeea1
Quelldatensatz
uspto-grants-2012_05
Patentnummer
US08183380B2

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