Hexadecylamine → N-hexadecyl-N'-propylsulfamide
Reaktionsgleichung
[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:18]([NH:21][S:22](Cl)(=[O:24])=[O:23])[CH2:19][CH3:20]>>[CH2:1]([NH:17][S:22]([NH:21][CH2:18][CH2:19][CH3:20])(=[O:24])=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]Komponenten
3
Versuchsvorschrift
The title compound was prepared following the method described in Example 6. The starting reactants are 0.15 g (0.6 mmol) of N-hexadecylamine and 0.10 g (0.6 mmol) of N-propylsulfamoyl chloride. 0.15 g of a white solid were obtained. Yield 70%; m.p. 108-110° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-c55cd12b4dad476ea629dd59b73d3c04
- Quelldatensatz
- uspto-grants-2012_05
- Patentnummer
- US08188312B2