Cobalt dinitrate → Iron cobalt bismuth nitrate

HRID 1934322

Reaktionsgleichung

[N+:1]([O-:4])([O-:3])=[O:2].[Fe+2:5].[N+:6]([O-:9])([O-:8])=[O:7].[N+:10]([O-:13])([O-:12])=[O:11].[Co+2:14].[N+:15]([O-:18])([O-:17])=[O:16].[N+:19]([O-:22])([O-:21])=[O:20].[Bi+3:23].[N+:24]([O-:27])([O-:26])=[O:25].[N+:28]([O-:31])([O-:30])=[O:29]>>[N+:1]([O-:4])([O-:3])=[O:2].[Bi+3:23].[Co+2:14].[Fe+2:5].[N+:6]([O-:9])([O-:8])=[O:7].[N+:10]([O-:13])([O-:12])=[O:11].[N+:15]([O-:18])([O-:17])=[O:16].[N+:19]([O-:22])([O-:21])=[O:20].[N+:24]([O-:27])([O-:26])=[O:25].[N+:28]([O-:31])([O-:30])=[O:29]

Komponenten

Edukt 3

HCID 25000Cobalt dinitrate

HCID 107711Bismuth nitrate

HCID 9815404Ferrous nitrate

Produkt 1

HCID 131723207Iron cobalt bismuth nitrate

Versuchsvorschrift

1191.4 g of iron nitrate (14.2% by weight of Fe) are added, while stirring, to 3427.6 g of a cobalt nitrate solution (12.4% by weight of Co) preheated to 60° C. After the end of the addition, stirring is continued for a further 30 minutes, the temperature being kept constant at 60° C. Finally, 1922.5 g of the bismuth nitrate solution (11.2% by weight of Bi) are added. Stirring is again continued for 10 minutes at 60° C.

Aufarbeitung

custompreheated to 60° C
additionAfter the end of the addition
custombeing kept constant at 60° C
stirringStirring
waitis again continued for 10 minutes at 60° C.

Quellen und Nachweise

ORD-Eintrag: ord-b169fe4308d34d58bac87162f40cbfcd
Quelldatensatz: uspto-grants-2002_05
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06383976B1

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