HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acid → 3-(4-Methoxyphenyl)-2-phenylpropionic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acid | HCID 236698 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | 3-(4-Methoxyphenyl)-2-phenylpropionic acid | HCID 97739 | — |
Reaktionsschritte
Palladium on activated carbon (10% wt., 2.77 g) was added to a solution of 3-(4-methoxyphenyl)-2-phenylacrylic acid (27.7 g, 0.11 mol) in acetic acid (1000 ml). The mixture was hydrogenated at ambient temperature. The mixture was filtered through Celite, and the solvent was evaporated. The product was recrystallized from a small amount of ethyl acetate. Melting point 220-221° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06388090B2 |
| Quelldatensatz | uspto-grants-2002_05 |
| ORD ID | ord-1882dce487974d0793678a129d3179de |
| Quellennotiz | uspto-grants-2002_05 |