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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1935734Erstellt: 26. Oktober 2026

3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acid → 3-(4-Methoxyphenyl)-2-phenylpropionic acid

https://huagongshe.com/reaction/1935734

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-(4-Methoxyphenyl)-2-phenylprop-2-enoic acidHCID 236698—
KatalysatorPalladiumHCID 23938—
LösungsmittelAcetic AcidHCID 176—
Produkt3-(4-Methoxyphenyl)-2-phenylpropionic acidHCID 97739—

Reaktionsschritte

Palladium on activated carbon (10% wt., 2.77 g) was added to a solution of 3-(4-methoxyphenyl)-2-phenylacrylic acid (27.7 g, 0.11 mol) in acetic acid (1000 ml). The mixture was hydrogenated at ambient temperature. The mixture was filtered through Celite, and the solvent was evaporated. The product was recrystallized from a small amount of ethyl acetate. Melting point 220-221° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06388090B2
Quelldatensatzuspto-grants-2002_05
ORD IDord-1882dce487974d0793678a129d3179de
Quellennotizuspto-grants-2002_05