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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1937084Erstellt: 26. Oktober 2026

Methyldichlorosilane → Monophenethyldichlorosilane

https://huagongshe.com/reaction/1937084

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyldichlorosilaneHCID 6376—
EduktBenzyl ChlorideHCID 7503—
EduktBenzyltributylphosphonium chlorideHCID 200231—
ProduktMonophenethyldichlorosilaneHCID 123907249240,6%

Reaktionsschritte

In the same apparatus and procedure as Example 1 above, 0.26 g (0.79 mmol) of benyltributylphosphonium chloride, 1.00 g (7.90 mmol) of benzyl chloride, and 2.73 g (23.7 mmol) of methyldichlorosilane were reacted at 200° C. for 2 hrs. The resulting mixture was distilled to give 0.39 g of benzylmethyldichlorosilane (yield; 24%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06392077B1
Quelldatensatzuspto-grants-2002_05
ORD IDord-84c2b1619e68493395844cfc4bd26695
Quellennotizuspto-grants-2002_05