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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1937085Erstellt: 26. Oktober 2026

Benzyl Chloride → Benzene, [(trichlorosilyl)methyl]-

https://huagongshe.com/reaction/1937085

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzyl ChlorideHCID 7503—
EduktDichlorosilaneHCID 61330—
EduktBenzyltributylphosphonium chlorideHCID 200231—
ProduktBenzene, [(trichlorosilyl)methyl]-HCID 6986353%
ProduktBenzyldichlorosilaneHCID 10194310219%

Reaktionsschritte

In the same apparatus and procedure as Example 1 above, 0.26 g (0.79 mmol) of benyltributylphosphonium chloride, 1.01 ml (7.98 mmol) of benzyl chloride, and 2.42 g (24.0 mmol) of dichlorosilane were reacted at 150° C. for 2 hrs. The resulting mixture was distilled to give 0.29 g of benzyldichlorosilane (yield; 19%) and 0.95 g of benzyltrichlorosilane (yield; 53%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06392077B1
Quelldatensatzuspto-grants-2002_05
ORD IDord-380bfbcecc3d4ac1a46bb07f1b202964
Quellennotizuspto-grants-2002_05