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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1937648Erstellt: 26. Oktober 2026

Acrylamide → n-Decylacrylamide Acrylamid

https://huagongshe.com/reaction/1937648

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcrylamideHCID 6579—
Edukt2-MethylidenedodecanamideHCID 21275879—
LösungsmittelIsopropanolHCID 3776—
Produktn-Decylacrylamide AcrylamidHCID 21275878—

Reaktionsbedingungen

Temperatur75 °C

Reaktionsschritte

To a 500 mL round-bottom, three-neck flask fitted with a thermocouple, reflux condenser, and septum was added 150 mL of isopropanol followed by 16.13 g of a 50% aqueous solution of 2-trimethylammoniumethylacrylate chloride, 8.06 g of n-decylacrylamide, and 8.06 g of acrylamide. The solution was purged with nitrogen for 1 hour and 0.5 g AIBN was added. The mixture was purged for ˜15 minutes until all of the AIBN dissolved. The solution was heated to 75° C. under nitrogen for 16 hours.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06395777B2
Quelldatensatzuspto-grants-2002_05
ORD IDord-75de3cdfc8b14e4385c206ef40134096
Quellennotizuspto-grants-2002_05