4-Phenylpiperazine-1-carboxylic acid (4,4-diethoxybutyl)amide → 4-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide

HRID 1942373Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1942373
C([O:3][CH:4](OCC)[CH2:5][CH2:6][CH2:7][NH:8][C:9]([N:11]1[CH2:16][CH2:15][N:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:13][CH2:12]1)=[O:10])C.O=CCCCNC(C1CCCCC1)=O>>[O:3]=[CH:4][CH2:5][CH2:6][CH2:7][NH:8][C:9]([N:11]1[CH2:12][CH2:13][N:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:15][CH2:16]1)=[O:10]

Komponenten

3

Edukt 2

HCID 669375364-Phenylpiperazine-1-carboxylic acid (4,4-diethoxybutyl)amideHCID 85725969Cyclohexanecarboxylic acid (4-oxo-butyl)-amide

Produkt 1

HCID 866513094-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide

Versuchsvorschrift

4-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide (61C) is prepared from 61B as described for 20B. The product is obtained in almost quantitative yield.

Aufarbeitung

  1. customThe product is obtained in almost quantitative yield

Quellen und Nachweise

ORD-Eintrag
ord-f3b89ee816344ddbbf4e68c4b58ff5cf
Quelldatensatz
uspto-grants-2013_03
Patentnummer
US08389555B2

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